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It could indicate bacterial contamination, that the peptide has not fully dissolved, or that it has crashed out of solution due to improper reconstitution or a pH issue

Oostenbrink C, Villa A, Mark AE, van Gunsteren WF (2004) A biomolecular force field based on the free enthalpy of hydration and solvation: the GROMOS force-field parameter sets 53A5 and 53A6

These include severe dysmenorrhea requiring prescription analgesics, progressive worsening of menstrual pain, pain occurring outside of menstruation, deep dyspareunia, and cyclic gastrointestinal or urinary symptoms (Kennedy et al., 2005)

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